Motofit corefines neutron and xray reflectometry data, using the abeles matrix parratt recursion and least squares fitting genetic algorithm or levenberg marquardt. Xray reflectivity xrr is a unique analysis technique for the nondestructive and calibration free investigation of structural properties of thin films down to the sub. Reflectometry is used to characterize single and multilayer structures and coatings in magnetic, semiconducting and optical materials, among others. What is the best fitting software for xrr measurements. Xray reflectometry, uvvis and ftirellipsometry and ftir.
Jgixa a software package for the calculation and fitting of grazing. X ray form factor, attenuation, and scattering tables nist. Interactive, webbased calculator of neutron and xray. Basic principles of xray reflectivity in thin films. Ncnr has a number of programs to aid in reflectometry. For many users of the neutron and xray reflectometry instruments at nist, these measurements represent a relatively small and specialized part of their research portfolio. Since neutron reflectometry is sensitive to contrast arising from different nuclei as compared to electron density, which is measured in xray scattering, q c is replaced by the neutron scattering. Xray reflectometry, grazing incidence small angle xray. The aim of this web page is to give a rapid but incomplete overview of the reflex program. Xray reflectivity sometimes known as xray specular reflectivity, xray reflectometry, or xrr is a surfacesensitive analytical technique used in chemistry, physics, and materials science to. Variableresolution xray reflectivity analysis of aln thin films on sapphire. Recent developments in the xray reflectivity analysis. Evaluation of uniformity of thin film thickness by xray reflectivity mapping.
Typically cu radiation is used with minimum resolution of 0. The thermo scientific arl equinox 5000 xray diffractometer is a multipurpose xrd instrument. There is also a downloadable app that can be used on android devices. Part of malvern panalyticals xrd software range, reflectivity uses the xrdml data format. In x ray reflectometry xrr analysis, the instrument reflects a beam of x rays on a flat surface and measures the intensity of x rays reflected in the specular direction reflected angle equal to incident angle. X ray reflectometry xrr is an analytical technique for investigating thin layered structures, surfaces and interfaces using the effect of total external reflection of x rays. Xray reflectometry xrr is an analytical technique for investigating thin layered structures, surfaces and interfaces using the effect of total external reflection of xrays. Analysing thin films and coatings with xray reflectometry. Diffractometer manufacturers typically provide commercial software to be used for xray reflectivity measurements. The ncnr xray diffractometer is configured to allow both. Xray reflectometry bruker d8 gadds allows a user to configure setup to meet the requirements to perform the xray reflectometry experiments.
The program is able to simulate standard nonmagnetic xray reflectivity. In xray reflectometry xrr analysis, the instrument reflects a beam of xrays on a flat surface and measures the intensity of xrays reflected in the specular direction reflected. Introduction bornagain is an opensource research software to simulate and fit neutron and xray reflectometry and grazingincidence smallangle scattering gisans and gisaxs. Reflection of x rays or neutrons provides a powerful means to study the structure and composition of thin films and interfacial layers. Sign up neutron and xray reflectometry analysis in. Xpert reflectivity is a software package for displaying, simulating and fitting xray reflectivity curves. Prescottb aansto, locked bag 2001, kirrawee dc, nsw 2232, australia, and bschool of chemical. The lab includes instrumentation for single crystal orientation analysis via realtime laue, in addition to reflectometry xrr, saxs, waxs and energydispersive xray fluorescence xrf. Xraycalc xray calc is a software for computer simulation of xray reflectivity, including normal incidence and grazing incidence xray reflectometry nixr and gixr. Reduction is driven by reflred, which allows you to view raw xray, ng1 and ng7 data files and reduce them to a. Xray reflectometry xrr thickness, density and roughness for multilayers on wafers when x rays are applied to a materials flat surface at grazing angles of incidence, total reflection will occur at or below a critical angle. It is cross platform and has been tested on linux, macos and windows.
Reductus is a web application providing support for data reduction and simple fitting of ncnr data. These web pages provide information about the use of neutron and x ray reflectivity. Xray and neutron reflectivity neutron science at ornl. In order to overcome this ambiguity, gixrf can be combined with xray reflectometry xrr. The dansereflectometry project is an nsf funded effort to. Reflex is a standalone software dedicated to the simulation and analysis of x rays and neutron reflectiity from multilayers implemented under matlab but it does. Xray reflectometry measurements of the samples were made at the australian nuclear science and technology organization ansto in sydney, australia, using a panalytical xpert pro. This training course will show the different methods used for xray reflectometry xrr and.
Renaud however, in general, the xray beam is incoherent over the sampled volume, so that only the average intensity is measured. Xray scattering spectroscopy is a powerful tool for investigations on rough surface and interface structures of multilayered thin film materials, 141 and xray. Welcome to, a website for neutron and xray reflectometry, and a little bit of triple axis spectrometry. Smartlab automated multipurpose xray diffractometer xrd with guidance software. A calculator for scattering length density that can be used for arbitrary x ray energies. It is specifically written for analysis of neutron data taken at multiple contrasts. Since neutron reflectometry is sensitive to contrast arising from different nuclei as compared to electron density, which is measured in x ray scattering, q c is replaced by the neutron scattering length density sld in reflex software. You can use our freeware program named reflex, which is a standalone program dedicated to the simulation and analysis of xray and neutron reflectivity. Reduction is driven by the reflred python libraries, which support the common operations required to convert raw x ray and neutron reflectivity data to a reflectivity curve in physical units. The running conditions for the xray tube are 40 kv and 40 ma, the power supply controls these with a stability of better than.
Xray reflectivity sometimes known as x ray specular reflectivity, x ray reflectometry, or xrr is a surfacesensitive analytical technique used in chemistry, physics, and materials science to characterize surfaces, thin films and multilayers. Its name, bornagain, alludes to the central role of the. It is used to determine layer thickness, density and roughness of thin layered samples. Xray analysis materials research lab university of. Opensource research software to simulate and fit neutron and xray reflectometry and grazingincidence smallangle scattering. Rascal is a matlab based application for the analysis of neutron and xray reflectivity data. As well as the scipy algorithms refnx uses the emcee affine invariant markov chain monte carlo.
Xray reflectometry xrr and grazing incidence diffraction gid wednesdaythursday, 9am4pm. Remagx is a scientific software to calculate and fit the specular xray. Reflection of xrays or neutrons provides a powerful means to study the structure and composition of thin films and interfacial layers. Xray reflectivity is a surfacesensitive analytical technique used in. Perform phase identification and quantification and structural analysis of polycrystalline materials. It is related to the complementary techniques of neutron reflectometry and ellipsometry. When an xray beam impinges on the surface of a sample, similar considerations apply as for optics with visible light, i.
Reflex is a standalone software dedicated to the simulation and analysis of xrays and neutron reflectiity from multilayers implemented under matlab but it does. Comparison of four data analysis software for combined x. Data processing software includes leptos and topaz. Jgixa a software package for the calculation and fitting of grazing incidence xray fluorescence and xray reflectivity data for the characterization of nanometerlayers and ultrashallowimplants. Xray reflectometry xrr is an analytical technique for investigating thin layered structures, surfaces and interfaces using the effect of total external reflection of x rays. X ray interactions with matter optical constants lawrence berkeley. Genx is a versitaile fitting software for xray and neutron reflectivity.
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